Chemistry

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Peter Fedoročko (ed.)

Proceedings of the 7th Annual Doctoral Spring School 2020

From November 10 to November 11, 2020, the 7th annual Spring School for Doctoral Students at Pavol Jozef Šafárik University in Košice will take place in Košice in a modified mode in the on-line space. The scientific program of the spring school will comprise 2 plenary lectures by leading scientific experts of Pavol Jozef Šafárik University in Košice. Doctoral students will present their research papers in two sections: 24 doctoral students of Faculty of Public Administration, Faculty of Law and Faculty of Arts, and 22 doctoral students of Faculty of Medicine and Faculty of Science.

The scientific programme of the spring school will also include a panel discussion with the management of Pavol Jozef Šafárik University in Košice.

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Jana Shepa - Ivana Šišoláková (eds.)

Abstracts of the 4th International Conference Nanomaterials: Fundamentals and Applications (NFA) 2020 is the contributions summary of the conference participants. The conference will feature three invited lectures and eight registered lectures. This conference is a tool for creating a dialogue between experts in the field of nanomaterials, their use and overall application in various fields. Papers in the proceedings are thematically divided into 6 areas. All contributions are highly professional and interesting and can contribute to further creative scientific work.

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Zuzana Orságová Králová (ed.)

The scientific book of abstracts is a summary of the contributions of teachers, scientists and other conference participants, which contain the original results of their scientific and research activities. Their work will be the subject of the next domestic conference „New Trends in Chemistry, Research and Education at Faculty of Science of P. J. Šafárik University in Košice 2020“. The conference is a space for dialogue between scientific academics on the one hand and professional staff and students on the other.

The contributions published in this volume can be divided according to content into the field of analytical, inorganic, physical, organic chemistry, biochemistry and didactics of chemistry. All contributions are interesting and can be used in further creative scientific and research work, in the process of education and in practical work.

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Juraj Černák

A significant part of inorganic chemistry is coordination chemistry, which deals with coordination compounds. Coordination compounds are numerous because they arise from the combination of central atoms, mostly metals, with ligands, and every organic compound is a potential ligand. This is confirmed by a recent report that American scientists M. Brookhart, C. Schauer, and their colleagues from universities in North Carolina and Washington described the preparation of a rhodium complex with methane as a ligand.

This textbook is based on the long-term experience of the author in teaching and testing this subject. The subject is well-covered in several textbooks of varying difficulty in English; their partial list can be found by readers in the list of used literature at the end of this textbook. On the other hand, in Slovak language, coordination chemistry issues are only marginally covered in several textbooks focused more on general inorganic chemistry but lack a comprehensive view on this topic. From this follows the goal of this proposed textbook - to cover the lack of study literature in this area for Slovak language.

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Veronika Niščáková - Ivana Šišoláková (eds.)

Abstracts of the 5th Intemational Conference Nanomaterials: Fundamentals and Applications (NF A) 2021 is the contributions summary of the conference participants. The conference will feature four invited lectures and ten registered lectures. This conference is a tool for creating a dialogue between experts in the field of nanomaterials, their use and overall application in various fields.

Papers in the proceedings are thematically divided into 6 areas. All contributions are highly professional and interesting and can contribute to further creative scientific work.

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Mária Kožurková (ed.)

Book of Abstracts

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Jana Shepa (ed.)

The book of abstracts from the second year of the international conference Spring electrochemical meeting is composed of contributions from the participants of this student conference.

The conference consisted of one invited lecture and ten competing student lectures. The message of this meeting is to create a dialogue between students of electrochemistry and the mutual exchange of knowledge. All contributions are professionally processed and inspiring.

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Monika Tvrdoňová, Miroslava Martinková

The scientific book of abstracts from conference „Novel Trends in Chemistry, Research and Education 2022“ is a summary of the contributions of conference participants, which contain the original results of their scientific and research activities. The contributions published in this volume can be divided according to content into the field of analytical, inorganic, organic, physical chemistry, biochemistry, didactics of chemistry and NMR spectroscopy.

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Jana Shepa (ed.)

The book of abstracts from 6th International Conference on Nanomaterials: Fundamentals and Applications, NFA 2022 is composed of contributions from the participants of this international conference. The conference consisted of 4 invited lecture and 52 abstracts of participants. The conference is focused on nanotechnology and its application in various research areas. All contributions are professionally processed and inspiring.

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Jozef Bednarčík

Crystallography deals with discerning the arrangement and bonding of atoms in crystalline solids. Almost immediately after their discovery, X-rays began to be used to study the internal structure of substances. The first chapter of this textbook deals with the basic concepts of crystallography. At the beginning, crystalline solids are characterized. In the next section, the basic types of bonds and their characteristics are briefly presented. The main subject of this chapter is the interpretation of basic concepts such as symmetry operations, translational periodicity, grid, elementary cell. Spatial lattices and crystal systems are presented. At the end of this chapter, attention is paid to the description of individual types of defects in crystal structures. In the second chapter, the Bohr model of the hydrogen atom is presented. Individual quantum numbers and their meaning are given. Next, energy levels and allowed transitions within an atom with multiple electrons are described. The second chapter concludes with the characterization of the basic absorption and emission processes. The third chapter is devoted to the production of X-ray radiation and its properties. Sources of X-ray radiation and a description of their operation are presented. Interaction of X-ray radiation with matter, absorption and detection of X-ray radiation are the subject of the last part of this chapter.

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Marián Kireš  (ed.)

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Peter Fedoročko (ed.)

From June 13 to June 16, 2023, the 9th annual Spring School for Doctoral Students at Pavol Jozef Šafárik University in Košice will take place in Stará Lesná. The scientific program of the spring school will comprise 3 plenary lectures by leading scientific experts and 1 workshop. Doctoral students will present their research papers in two sections: 24 doctoral students of Faculty of Public Administration, Faculty of Law and Faculty of Arts, and 24 doctoral students of Faculty of Medicine and Faculty of Science. The scientific programme of the spring school will also include a panel discussion with the management of Pavol Jozef Šafárik University in Košice.

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Ivana Šišoláková - Radka Gorejová - Jana Shepa - Renáta Oriňaková

The university textbook "Advanced Electrochemical Methods" is a teaching aid intended for master's or doctoral students studying electrochemical subjects at the Department of Physical Chemistry, Faculty of Science, Pavol Jozef Šafárik University in Košice. These textbooks follow and further develop textbooks focused on the basic electrochemical methods currently used in modern research. The presented teaching texts are processed in sixteen clear chapters, where they provide a theoretical principle and derivation of electrochemical processes and mechanisms in individual methods. Teaching texts also consist of practical laboratory exercises, in which students can try out the real application of the studied electrochemical methods. The practical tasks are focused primarily on the demonstration of research that is carried out at our workplace. Students will be able to try, for example, electrochemical modification of the electrode surface, preparation of electrochemical sensors for the determination of analytes, preparation and characterization of a dye-sensitized solar cell or electrochemical evolution of hydrogen.

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Lucia Andrezálová, Zdeňka Ďuračková,Mária Chomová,Vladimír Jakuš, Miriam Ježovičová, Jana Muchová, Zuzana Országhová,Ingrid Žitňanová

Chemistry and biochemistry at medical faculties are integral parts of basic theoretic knowledge of contemporary graduate. Educational book “Textbook of Medical Chemistry” is destined to students of study branches General Medicine and Dentistry for the course “Medical Chemistry”. It is structured into 13 chapters concerning several topics: general and physical chemistry, organic chemistry, chemistry of natural substances (static biochemistry), enzymology and oxidative stress. Individual chapters provide comprehensible explanation of the fundamentals of physico-chemical, chemical and biochemical relationships applying in living systems as well as the knowledge of the structure of biologically important molecules (simple molecules and macromolecules) related to their properties and biological function.

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Miroslav Almáši

The scientific book of abstracts from the conference „Novel Trends in Chemistry, Research and Education 2023“ is a summary of the contributions of conference participants, which contain the original results of their scientific and research activities. The contributions published in this volume can be divided according to content into the fields of analytical, inorganic, organic, physical chemistry, biochemistry, didactics of chemistry, and NMR spectroscopy.

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Jana Shepa (ed.)

The book of abstracts from 7th International Conference on Novel Materials: Fundamentals and Applications, NFA 2023 is composed of contributions from the participants of this international conference. The conference consisted of 3 invited lecture and 40 abstracts of participants. The conference is focused on novel materials and its application in various research areas. All contributions are professionally processed and inspiring.

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Miroslava Martinková

This electronic material provides the basic principles of creating a systematic nomenclature of organic compounds, from the simplest hydrocarbons to the more complicated nomenclature of carbohydrates. For some groups of derivatives, alternative ways of generating system names are also mentioned, as well as the most common trivial names that are still in use in the literature and in practice, in some cases being the characteristic (dominant) ones. In the introductory section, the basic rules to be respected when writing names of organic compounds are discussed. This document is intended primarily for interdisciplinary undergraduate and graduate students as support material for the courses Organic Chemistry and Selected Chapters in Organic Chemistry and Biochemistry. In the final section of this document, solved examples are given so that the student can check how the rules for forming the names of organic compounds have been understood.

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Miroslava Martinková

This electronic material focuses on the subject of secondary metabolism and its products - secondary metabolites. The material gives an overview of the basic building blocks and construction mechanisms through which molecules can be synthesized in living organisms (plants). The processes of formation of the mentioned metabolites are explained using the basic mechanisms of organic reactions. Several of the secondary metabolites presented have a remarkable biological profile and are used as therapeutics or serve as lead compounds for the development of novel pharmacological agents. This electronic document is primarily intended for students of the Master's degree programme in Organic Chemistry as supporting material for the profile subject Chemistry of Natural Products.

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Slávka Hamuľaková

The textbook "Structure and reactivity - solved examples and tasks, part 1" is the basis for teaching the subject "Structure and reactivity" for students of the 1st year of master's studies at the Faculty of Science, UPJŠ, department of Organic Chemistry. The textbook is divided into individual chapters, each chapter offering students examples of chemical reactions, where their course is explained on the basis of appropriate reaction mechanisms. A substantial part of the textbook consists of unresolved tasks, the main goal of which is the development of students' knowledge and skills. Due to the fact that the textbook is focused on only one semester of study, it cannot cover all reactions, rather it is only representative examples of different types of reactions, such as: addition reactions, elimination reactions, aromatic substitution, addition-elimination reactions, radical reactions and pericyclic reactions.

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Ivana Sotáková-Martin Vavra-Mária Ganajová

This textbook has been designed for the master students of chemistry teaching (combined) at the Faculty of Science, Pavol Jozef Šafárik University in Košice as a source of model school experiments in general and inorganic chemistry. It will be used for teaching the Special Practice of School Experiments I compulsory course. It consists of instructions for experiments related to the selected topics in general and inorganic chemistry as well as the didactic and technical aspects of their performance. Each experiment includes an explanation of the principle, specification of the tools and chemicals needed, working procedure, and the respective apparatus assembly scheme. At the end of each experiment, the observation and explanation necessary for the correct interpretation of the results of the chemical experiment performed are provided. To follow the requirements for the digital transformation of education, selected computer-aided experiments and visualiser projections have been included as well. The next part is focused on the work with the monitoring suitcase, which can be used for making simple field experiments related to environmental topics. The final part is dedicated to attractive experiments that complement the topics in inorganic chemistry and can be used to motivate students. All experiment instructions are in line with the requirements specified by the state educational programmes for primary and grammar schools. This book allows teachers to select appropriate demonstrative experiments or experiments for laboratory classes performed by students themselves. The videos of selected experiments are also available as part of the interactive periodical table of elements operated by the Institute of Chemistry, Faculty of Science, Pavol Jozef Šafárik University in Košice.

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Nataša Tomášková

Selected tasks and problems from biochemistry – metabolism follow biochemistry lectures on metabolism and individual metabolic pathways for students of the second and third year of the bachelor’s degree in the fields of chemistry, biology and their combinations with other fields. Scripts provide an opportunity to better understand the lectured subject matter of metabolism through the solution of tasks and problems as serve as a basis for one-hour exercises. The scripts are divided thematically into eleven chapters, and each chapter contains 10 tasks and 7 problems. At the beginning of the chapters there is a short description and explanation of the given metabolic pathway. However, when solving the tasks, the student must focus mainly on the curriculum that was presented on the given topic in the lecture. Subsequently, at the end of chapter, answers to problems are also presented. These scripts are intentionally accessible only in electronic form. The reason is the effort to continuously update and modernize individual tasks.

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Mária Vilková - Zuzana Kudličková - Ján Elečko

Organic chemistry is the chemistry of carbon. Organic compounds in the form of large molecules (macromolecules), such as nucleic acids, proteins, carbohydrates, and lipids are the basic elements of living organisms. This study material is created for non-chemistry students, especially students of biology. Most of these students have little or no knowledge of organic chemistry. Therefore, we proceed from the basic principles of organic chemistry to biochemistry.

The basic principles of organic chemistry and biochemistry are briefly summarized in individual chapters, but the main content consists of tasks for practising basic knowledge. To check the correctness of solving the tasks, the correct solutions are also given. The importance of this study material lies in the fact that students will get additional study material that they will use in studying the subject Basics of Chemistry.

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Jana Shepa  (ed.)

The book of abstracts from 8th International Conference on Novel Materials: Fundamentals and Applications, NFA 2023 is composed of contributions from the participants of this international conference. The conference consisted of 6 invited lecture and 38 abstracts of participants. The conference is focused on novel materials and its application in various research areas. All contributions are professionally processed and inspiring.

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Miroslav Almáši (ed.)

The book of abstracts from the conference "Porous Materials for Environmental Applications 2024" is a collection of contributions of the conference participants, which contain original results of their scientific and research activities. The conference was aimed to share new findings dealing with the preparation, characterization and application of porous materials in environmental fields.

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Marián Kireš - Renáta Orosová a kol.

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Ivana Šišoláková (ed.)

The book of abstracts from the international conference Spring Electrochemical Meeting is composed of contributions from the participants of this conference. The conference consisted of two invited lectures and four other lectures. The event was focused on the sharing new knowledge in the field of electrochemistry connection with student part of this conference.

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Jana Šandrejová - Andrea Gajdošová (eds.)

The scientific book of abstracts from the conference „Novel Trends in Chemistry, Research and Education 2024“ is a summary of the contributions of conference participants, which contain the original results of their scientific and research activities. The contributions published in this volume are divided according to content into the fields of analytical, inorganic, organic, physical chemistry, biochemistry and didactics of chemistry.

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Zuzana Jurašeková

Úvod k praktikám k experimentálnym metódam biofyziky

The university textbook titled Laboratory Techniques and Calculations is designed for the first-year students of the bachelor's degree in Biophysics at the Institute of Physics, Faculty of Sciences, P. J. Šafárik University in Košice. The objective is to equip students with fundamental knowledge and practical skills for the work in a chemical laboratory. It is essential for addressing different biophysical issues and experiments that students will have to solve later. The textbook comprises three principal sections: a theoretical part focused on the calculations, a section dedicated to laboratory work, and the last part offers a brief introduction to spectroscopy. The theoretical part summarizes the basic definitions and equations related to the characterization and preparation of solutions and mixtures. The second, most comprehensive part provides guidance and suggestions for safe and efficient practices in a chemical laboratory. The primary focus is on the manipulation of chemical substances and the use of specific small laboratory instruments and equipment. The fundamental laboratory procedure guides for the selected laboratory works are also provided. As part of a short introduction to spectroscopy, students can become familiar with fundamental spectroscopic concepts and principles. UV-VIS absorption spectrophotometry receives special attention, along with a brief introduction to fluorescence. The textbook is supplemented by various practical and theoretical tasks, as well as numerous web links to further explanatory texts and videos.

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Daniel Jancura - Erik Sedlák

The textbook "Bioenergetics" should serve as an introduction to the study of bioenergetics. This field of science is currently highly actual, as the results of the bioenergetics research in recent years clearly show that bioenergetics processes in living systems can "serve" not only to transformation of energy, but also affect the course of processes such as apoptosis, aging, origin and development of many diseases (especially neurodegenerative).

These facts clearly indicate the need for the existence of quality teaching texts that would allow students to acquire the necessary information and knowledge in this scientific discipline in an acceptable way. For the above mentioned reasons, we decided to create these textbooks, which are in the form of ten chapters, which naturally and logically follow each other. 

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Andrea Morovská Turoňová - Renáta Oriňaková - František Kaľavský 

The university textbooks "Practical Exercises in Physical Chemistry" are intended as teaching literature for students of the 2nd year of the Chemistry study program and the 3rd year of the interdisciplinary study program at the Faculty of Science of the Pavel Jozef Šafárik University in Košice.

The three chapters summarize the basic knowledge of thermodynamics, electrochemistry and kinetics, the next chapter deals with the measurement of some other physico-chemical quantities. The tasks developed on the basis of cooperation with the Criminalistics and Expertise Institute of the Police in Košice, which also participates in the innovation of practical teaching, are also very attractive and interesting for students. Thematic units are updated and supplemented by new knowledge, principles as well as detailed working procedures using new instrumentation.

The aim of laboratory exercises in physical chemistry is to illustrate and confirm the physicochemical laws and correlations that apply to the quantitative description of chemical phenomena. Students will learn to use instruments and equipment that occur in physico-chemical laboratories, they will learn the principles of accurate and correct quantitative measurement of physical quantities, important from a chemical point of view. They can also develop professional and scientific communication skills, and we want to support their creative approach to making measurement protocols.

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Jana Shepa (ed.)

The book of abstracts from the first year of the international conference Autumn electrochemical meeting is composed of contributions from the participants of this student conference.

The conference consisted of one invited lecture and six student lectures. The message of this meeting is to create a dialogue between students of electrochemistry and the mutual exchange of knowledge. All contributions are professionally processed and inspiring.

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E-book

Mária Vilková - Zuzana Kudličková - Aneta Salayová - Tomáš Ján Liška

The Nuclear Magnetic Resonance Practicum – Part 1: Quantitative NMR is designed for students taking the NMR Practicals course, which focuses on the practical aspects of quantitative nuclear magnetic resonance (qNMR). This publication builds on previous NMR courses and assumes basic theoretical knowledge of the method, emphasizing experimental procedures, data processing, and result interpretation. qNMR is a precise analytical technique with broad applications in analytical chemistry, pharmaceutical research, biomedicine, and quality control. The script provides a detailed guide to conducting experiments, as well as procedures for analyzing and evaluating acquired data. This publication offers students methodological guidance and support in mastering qNMR analysis and serves as a valuable resource not only during their studies but also for further research in NMR spectroscopy.

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