Vybrané experimentálne úlohy z koloidiky

E-book

Ľubomír Antoni-Stanislav Krajči

An important part of theoretical computer science is the problem of Turing machines. This computational model has two basic properties: like any other computational program, the software of a Turing machine is composed of instructions, but in its case they are all of a single type. Every other (so far known) computer program can be transformed into a Turing machine program without loss of information. While the second feature reduces the question of what a calculator cannot do to the question of what a Turing machine cannot do, the first feature allows a much simpler investigation of such a question. Using this computational model, we can thus find concrete problems that no automaton can ever deal with (perhaps the most famous is the problem of the Turing machine stopping). Their existence demonstrates the fundamental limitations of (not only ideal) computational means, and thus encourages both criticality and humility in our thinking.

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E-book

Karel Saksl

Solving crystal structures is the royal discipline of X-ray crystallography. Its primary task, with the exception of defects, is to describe the atomic structure of the motif that, by its repetition, fills the volume of the entire crystal or crystalline phase. This task is nowadays more or less routine for single-crystal X-ray diffraction, which can locate hundreds to thousands of non-hydrogen atoms in large unit cells. However, in real practice, we often have material available only in powder form instead of single crystals. Solving the atomic structure from its X-ray diffraction data is non-trivial, mainly because the three-dimensional diffraction space of a single crystal is reduced to one dimension by measuring a large number of randomly oriented microcrystals (crystallites). Therefore, the solution itself requires, in addition to proper measurement methodology, the selection of suitable tools, procedures, and strategies that, through optimization, will lead to the solution and refinement of the given crystalline phase. The current limit of this method is approximately 100 non-hydrogen atoms in the asymmetric part of the unit cell, which, however, is sufficient for most inorganic materials.

The goal of these educational texts is to provide students in the second and third levels of university studies with specific guidance on solving crystal structures from powder X-ray diffraction data. These scripts build upon my first monograph and require practical knowledge of its content. Similar to my previous monograph, I offer solved examples without a deep theoretical introduction, demonstrating procedures and strategies leading to the correct solution of crystalline phases using the freely available GSAS-II program. The examples are arranged from simpler to more complex, and the reader will find many useful pieces of information in the literature references as well as in the comments below the line. Part of these scripts are data intended for your individual practice of the described procedures. 

Karel Sakls

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E-book

Erik Čižmár

The textbook "Special Practicum II" is dedicated to describing experimental methods used for studying the magnetic properties of solid materials, especially low-dimensional and molecular magnets. It subsequently contains instructions for the practical exercise "Special Practicum II," during which master's and doctoral students use state-of-the-art commercial equipment-an electron paramagnetic resonance (EPR) spectrometer and a SQUID magnetometer.

The introductory chapter briefly describes the origin of magnetism in solids, the role of the crystal field, and magnetic interactions in explaining their magnetic properties. This is followed by an explanation of the principles of EPR, the operation of the EPR spectrometer, and the optimization of its parameters for the specific practical exercise.

The next part of the textbook is devoted to an overview of the behavior of magnetic quantities with changes in magnetic field or temperature in various types of magnets. The textbook concludes with a description of the operating principle of the SQUID magnetometer and an example of its use in a practical exercise measuring the magnetic moment.

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E-book

Erik Sedlák - Rastislav Varhač -  Patrik Danko - Helena Paulíková - Dušan Podhradský

The presented scripts were created in an effort to update and especially clarify the tasks that are solved in the basic practical exercises in biochemistry students of the 2nd and 3rd year of the bachelor's degree in chemistry, biology and their combinations with other disciplines. Most of the tasks come from the original scripts "Podhradský, Mihalovová: Praktické cvičenia z biochémie, Košice 1989".

Some of them have been modified to a greater or lesser extent and adapted to current conditions in the laboratory. New tasks were also added, such as those dedicated to nucleic acids. The scripts are thematically divided into six separate units, each of which consists of several tasks. The names of the units correspond to the nature of the biomacromolecules, which form their central theme. Theoretical introductions at the beginning of the unit are newly constructed and their main goal is to provide a brief overview of the basic biochemical methods used in the study of biomacromolecules.

These scripts are intentionally only available in electronic form. The reason is the effort to continuously update and modernize individual tasks according to the changing possibilities of our laboratory. We hope that the scripts will fulfill their role and that students will have sufficient theoretical knowledge and practical skills in the field of basic biochemical methods after completing these laboratory exercises.

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 Matúš Harminc 

Tento učebný text je určený poslucháčom medziodborového štúdia v kombináciách s matematikou, jednoodborového štúdia matematiky ako aj rozširujúceho štúdia matematiky. Je za-meraný na kvadratické kongruencie a niektoré diofantovské rovnice.

Autor

E-book

Renáta Oriňáková (ed.)

Book of abstract

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E-book

Gregor Bánó

Photonics is an application-oriented discipline at the interface of optics, opto-electronics and quantum optics. It includes classical optics extended by the description of physical phenomena and optical devices that rely on quantum (photon) nature of light.
The main objective of the Photonics course is to provide a comprehensive overview of essential optical and photonic phenomena routinely applied in experimental scientific research while working with various light sources (e.g. in the field of biophotonics). The first chapters are devoted to the description of light at different levels. The logical order of subsections in this part corresponds to the structure of the textbook: B. E. A. Saleh, M. C. Teich, Fundamentals of Photonics. The following chapters contain a description of laser operation and an overview of selected optical instruments and their applications.
The body text is complemented by practical notes on the use of theoretical knowledge during daily work in the laboratory. The course of Photonics requires a basic knowledge of mathematics, electromagnetism and optics, and thus it is recommended to students who previously passed through the courses of the Bachelor's program in Physics.

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Mariana Budovská

The aim of writing the university textbook "Selected Heterocyclic Compounds" was to create a study aid for students of the Organic Chemistry program, which provides essential information in a clear format for the subject of Heterocyclic Compounds. In selecting the content of the textbook, the goal was to present basic information about the chemistry of the most significant heterocycles. Given that the summary of chemical knowledge about heterocycles is vast, it was not possible to include all heterocyclic compounds in the content.

The intention was for readers to orient themselves in the field of heterocyclic compounds. Separate chapters included in the content address the nomenclature of heterocycles, basic chemical properties of individual heterocycles, their synthesis and reactions, the occurrence of heterocycles in nature, and their practical applications (medications, dyes, pesticides, detergents, etc.).

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Ondrej Hutník (ed.)

Book of abstract

Uncertainty Modeling 2024 (UM 2024) is organized by Pavol Jozef ˇSaf´arik University in Koˇsice. It is a continuation of the series of colloquia held in Rzesz´ow under the name International Symposium on Fuzzy Sets (ISFS) and in Bratislava under the name Uncertainty Modeling.

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Monika Tvrdoňová - Miroslava Martinková

The scientific book of abstracts from conference „Novel Trends in Chemistry, Research and Education 2022“ is a summary of the contributions of conference participants, which contain the original results of their scientific and research activities. The contributions published in this volume can be divided according to content into the field of analytical, inorganic, organic, physical chemistry, biochemistry, didactics of chemistry and NMR spectroscopy.

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Igor Hudec - Ľubomír Kováč 

The study course provides the basic knowledge on the fundamental parameters, relationships and processes in ecological sciences. Brief content: ecological factors and relations to environment (air, water, soil); influence of ecological factors upon organisms (morphological adaptations, behavioural responses); populations and communities (external and internal parameters of populations, population dynamics); ecosystems (impact assessment) and biomes (basic features and human impact); cycles (hydrologic, gaseous, sedimentation) of basic elements on Earth.  

Authors

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Jana Shepa (ed.)

The book of abstracts from 6th International Conference on Nanomaterials: Fundamentals and Applications, NFA 2022 is composed of contributions from the participants of this international conference. The conference consisted of 4 invited lecture and 52 abstracts of participants. The conference is focused on nanotechnology and its application in various research areas. All contributions are professionally processed and inspiring.

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Veronika Niščáková - Ivana Šišoláková (eds.)

Abstracts of the 5th Intemational Conference Nanomaterials: Fundamentals and Applications (NF A) 2021 is the contributions summary of the conference participants. The conference will feature four invited lectures and ten registered lectures. This conference is a tool for creating a dialogue between experts in the field of nanomaterials, their use and overall application in various fields.

Papers in the proceedings are thematically divided into 6 areas. All contributions are highly professional and interesting and can contribute to further creative scientific work.

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Marián Kireš - Renáta Orosová a kol.

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Andrea Morovská Turoňová - Renáta Oriňaková - František Kaľavský 

The university textbooks "Practical Exercises in Physical Chemistry" are intended as teaching literature for students of the 2nd year of the Chemistry study program and the 3rd year of the interdisciplinary study program at the Faculty of Science of the Pavel Jozef Šafárik University in Košice.

The three chapters summarize the basic knowledge of thermodynamics, electrochemistry and kinetics, the next chapter deals with the measurement of some other physico-chemical quantities. The tasks developed on the basis of cooperation with the Criminalistics and Expertise Institute of the Police in Košice, which also participates in the innovation of practical teaching, are also very attractive and interesting for students. Thematic units are updated and supplemented by new knowledge, principles as well as detailed working procedures using new instrumentation.

The aim of laboratory exercises in physical chemistry is to illustrate and confirm the physicochemical laws and correlations that apply to the quantitative description of chemical phenomena. Students will learn to use instruments and equipment that occur in physico-chemical laboratories, they will learn the principles of accurate and correct quantitative measurement of physical quantities, important from a chemical point of view. They can also develop professional and scientific communication skills, and we want to support their creative approach to making measurement protocols.

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Jana Šandrejová - Andrea Gajdošová (eds.)

The scientific book of abstracts from the conference „Novel Trends in Chemistry, Research and Education 2024“ is a summary of the contributions of conference participants, which contain the original results of their scientific and research activities. The contributions published in this volume are divided according to content into the fields of analytical, inorganic, organic, physical chemistry, biochemistry and didactics of chemistry.

Download the e-book for free (pdf)

E-book

Ľubomír Antoni-Stanislav Krajči

An important part of theoretical computer science is the problem of Turing machines. This computational model has two basic properties: like any other computational program, the software of a Turing machine is composed of instructions, but in its case they are all of a single type. Every other (so far known) computer program can be transformed into a Turing machine program without loss of information. While the second feature reduces the question of what a calculator cannot do to the question of what a Turing machine cannot do, the first feature allows a much simpler investigation of such a question. Using this computational model, we can thus find concrete problems that no automaton can ever deal with (perhaps the most famous is the problem of the Turing machine stopping). Their existence demonstrates the fundamental limitations of (not only ideal) computational means, and thus encourages both criticality and humility in our thinking.

Download e-book for free (pdf)

E-book

Karel Saksl

Solving crystal structures is the royal discipline of X-ray crystallography. Its primary task, with the exception of defects, is to describe the atomic structure of the motif that, by its repetition, fills the volume of the entire crystal or crystalline phase. This task is nowadays more or less routine for single-crystal X-ray diffraction, which can locate hundreds to thousands of non-hydrogen atoms in large unit cells. However, in real practice, we often have material available only in powder form instead of single crystals. Solving the atomic structure from its X-ray diffraction data is non-trivial, mainly because the three-dimensional diffraction space of a single crystal is reduced to one dimension by measuring a large number of randomly oriented microcrystals (crystallites). Therefore, the solution itself requires, in addition to proper measurement methodology, the selection of suitable tools, procedures, and strategies that, through optimization, will lead to the solution and refinement of the given crystalline phase. The current limit of this method is approximately 100 non-hydrogen atoms in the asymmetric part of the unit cell, which, however, is sufficient for most inorganic materials.

The goal of these educational texts is to provide students in the second and third levels of university studies with specific guidance on solving crystal structures from powder X-ray diffraction data. These scripts build upon my first monograph and require practical knowledge of its content. Similar to my previous monograph, I offer solved examples without a deep theoretical introduction, demonstrating procedures and strategies leading to the correct solution of crystalline phases using the freely available GSAS-II program. The examples are arranged from simpler to more complex, and the reader will find many useful pieces of information in the literature references as well as in the comments below the line. Part of these scripts are data intended for your individual practice of the described procedures. 

Karel Sakls

Download the e-book for free  (pdf)

E-book

Erik Čižmár

The textbook "Special Practicum II" is dedicated to describing experimental methods used for studying the magnetic properties of solid materials, especially low-dimensional and molecular magnets. It subsequently contains instructions for the practical exercise "Special Practicum II," during which master's and doctoral students use state-of-the-art commercial equipment-an electron paramagnetic resonance (EPR) spectrometer and a SQUID magnetometer.

The introductory chapter briefly describes the origin of magnetism in solids, the role of the crystal field, and magnetic interactions in explaining their magnetic properties. This is followed by an explanation of the principles of EPR, the operation of the EPR spectrometer, and the optimization of its parameters for the specific practical exercise.

The next part of the textbook is devoted to an overview of the behavior of magnetic quantities with changes in magnetic field or temperature in various types of magnets. The textbook concludes with a description of the operating principle of the SQUID magnetometer and an example of its use in a practical exercise measuring the magnetic moment.

Download the e-book for free (pdf)

E-book

Erik Sedlák - Rastislav Varhač -  Patrik Danko - Helena Paulíková - Dušan Podhradský

The presented scripts were created in an effort to update and especially clarify the tasks that are solved in the basic practical exercises in biochemistry students of the 2nd and 3rd year of the bachelor's degree in chemistry, biology and their combinations with other disciplines. Most of the tasks come from the original scripts "Podhradský, Mihalovová: Praktické cvičenia z biochémie, Košice 1989".

Some of them have been modified to a greater or lesser extent and adapted to current conditions in the laboratory. New tasks were also added, such as those dedicated to nucleic acids. The scripts are thematically divided into six separate units, each of which consists of several tasks. The names of the units correspond to the nature of the biomacromolecules, which form their central theme. Theoretical introductions at the beginning of the unit are newly constructed and their main goal is to provide a brief overview of the basic biochemical methods used in the study of biomacromolecules.

These scripts are intentionally only available in electronic form. The reason is the effort to continuously update and modernize individual tasks according to the changing possibilities of our laboratory. We hope that the scripts will fulfill their role and that students will have sufficient theoretical knowledge and practical skills in the field of basic biochemical methods after completing these laboratory exercises.

Download e-book for free (pdf)

 Matúš Harminc 

Tento učebný text je určený poslucháčom medziodborového štúdia v kombináciách s matematikou, jednoodborového štúdia matematiky ako aj rozširujúceho štúdia matematiky. Je za-meraný na kvadratické kongruencie a niektoré diofantovské rovnice.

Autor