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Jozef Bednarčík (ed.)

The SFEL school is continuation of the Winter Schools of Synchrotron radiation held in 2011, 2013, 2014 and SFEL 2017, 2018 and 2019. All schools of the series were held here, in Liptovský Ján, where our conference venue offers conditions for friendly and creative atmosphere.

The aim of the SFEL 2022 school is to facilitate the growth of a new Slovak research community with high expertise in the area of high-efficiency RTG laser, synchrotron and neutron sources. The SFEL school is designed for efficient transfer of the rapidly developing know-howin these areas to young generation – researchers and university students. The next aim of the SFEL2022 is strengthening of personal connections between the local Slovak research community and actually forming scientific teams of XFEL users, scientific teams of synchrotron or neutron sources users, respectively.

Slovak research community thus can take advantage of the fact that Slovakia is a shareholder of the European XFEL GmbH company in Hamburg, but also makes more efficient use of other closely related scientific facilities, including ILL and ESRF in Grenoble and DESY in Hamburg.

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Miroslav Repčák - Martin Bačkor - Peter Paľove-Balang - Silvia Gajdošová

The establishment of the Plant Physiology Laboratory at the Department of Botany, Faculty of Arts, Pavol Jozef Šafárik University in Košice in 1969 was associated with the name of Ing. Štefan Kocúrik, CSc. (1923–2006), who also prepared the first "Instructions for Exercises in Plant Physiology" (Košice 1972, 1976).

Since 1980, the manual by Associate Professor RNDr. Karol Erdelský, CSc., and Ing. Fridrich Frič, DrSc., titled "Practicum and Analytical Methods in Plant Physiology" (Bratislava 1980) has been used. With the increase in the number of students, it became relevant in 1991 to publish the "Instructions for Exercises in Plant Physiology" again to improve preparation and the efficient organization of practical work. Associate Professor RNDr. A. Košturiak, CSc., contributed significantly to the expansion of the introductory part of the instructions with his valuable advice, for which the authors are grateful. For the fourth edition, some tasks were updated and modernized, taking into account the possibilities of the renovated laboratory. The selection of tasks was adapted to the current scope of exercises for individual plant physiology subjects within the bachelor's and master's study programs in biology and ecology. These subjects include: Plant Physiology, Plant Metabolism, Mineral Nutrition of Plants, Plant Growth and Development, and Plant Ecology. Some tasks are also suitable for high school experiments.

The choice of topics was influenced by the research focus of our workplace on secondary metabolism, ecophysiology, and medicinal plants. The instructions generally adhere to the SI unit system, occasionally including other commonly used units.

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Karel Saksl

Solving crystal structures is the royal discipline of X-ray crystallography. Its primary task, with the exception of defects, is to describe the atomic structure of the motif that, by its repetition, fills the volume of the entire crystal or crystalline phase. This task is nowadays more or less routine for single-crystal X-ray diffraction, which can locate hundreds to thousands of non-hydrogen atoms in large unit cells. However, in real practice, we often have material available only in powder form instead of single crystals. Solving the atomic structure from its X-ray diffraction data is non-trivial, mainly because the three-dimensional diffraction space of a single crystal is reduced to one dimension by measuring a large number of randomly oriented microcrystals (crystallites). Therefore, the solution itself requires, in addition to proper measurement methodology, the selection of suitable tools, procedures, and strategies that, through optimization, will lead to the solution and refinement of the given crystalline phase. The current limit of this method is approximately 100 non-hydrogen atoms in the asymmetric part of the unit cell, which, however, is sufficient for most inorganic materials.

The goal of these educational texts is to provide students in the second and third levels of university studies with specific guidance on solving crystal structures from powder X-ray diffraction data. These scripts build upon my first monograph and require practical knowledge of its content. Similar to my previous monograph, I offer solved examples without a deep theoretical introduction, demonstrating procedures and strategies leading to the correct solution of crystalline phases using the freely available GSAS-II program. The examples are arranged from simpler to more complex, and the reader will find many useful pieces of information in the literature references as well as in the comments below the line. Part of these scripts are data intended for your individual practice of the described procedures. 

Karel Sakls

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Ivan Potočňák

The script is a study literature for the subject Chemical Calculations, which is a mandatory course in the bachelor's degree programs in Chemistry and Chemistry – Interdisciplinary Studies, first year. The script contains 10 chapters with a total of 207 pages, guiding students through solved and unsolved examples to help them understand the subject matter.

Author

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