Metódy prípravy nanoštruktúr I

E-book

Nataša Tomášková

Selected tasks and problems from biochemistry – metabolism follow biochemistry lectures on metabolism and individual metabolic pathways for students of the second and third year of the bachelor’s degree in the fields of chemistry, biology and their combinations with other fields. Scripts provide an opportunity to better understand the lectured subject matter of metabolism through the solution of tasks and problems as serve as a basis for one-hour exercises. The scripts are divided thematically into eleven chapters, and each chapter contains 10 tasks and 7 problems. At the beginning of the chapters there is a short description and explanation of the given metabolic pathway. However, when solving the tasks, the student must focus mainly on the curriculum that was presented on the given topic in the lecture. Subsequently, at the end of chapter, answers to problems are also presented. These scripts are intentionally accessible only in electronic form. The reason is the effort to continuously update and modernize individual tasks.

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E-book

Jozef Bednarčík (ed.)

Pavol Jozef Šafárik University in Košice under the auspices of Ministry of Education, Research, Development and Youth of the Slovak Republic, Ministry of Economy of the Slovak Republic and European X-Ray Free-Electron Laser Facility GmbH in Hamburg organizes School of XFEL and Synchrotron Radiation Users 2024 (SFEL 2024). The school is continuation of the Winter Schools of Synchrotron radiation held in 2011, 2013, 2014 and SFEL 2017, 2018, 2019 and 2022. The aim of the SFEL2024 school is to facilitate the growth of new Slovak research community of high expertise in high-efficiency RTG laser and synchrotron and neutron sources. The SFEL school is designed for efficient transfer of the rapidly developing know-how in these areas to young generation – researchers and university students. The next aim of the SFEL2024 is strengthening of personal connections between the local Slovak research community and forming scientific teams of XFEL users. Slovak research community thus can take advantage of the fact that Slovakia is a shareholder of European XFEL GmbH Company in Hamburg, but also makes more efficient use of other closely related scientific facilities, including ILL and ESRF in Grenoble and DESY in Hamburg.

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Ivana Šišoláková - Radka Gorejová - Jana Shepa - Renáta Oriňaková

The university textbook "Advanced Electrochemical Methods" is a teaching aid intended for master's or doctoral students studying electrochemical subjects at the Department of Physical Chemistry, Faculty of Science, Pavol Jozef Šafárik University in Košice.

These textbooks follow and further develop textbooks focused on the basic electrochemical methods currently used in modern research. The presented teaching texts are processed in sixteen clear chapters, where they provide a theoretical principle and derivation of electrochemical processes and mechanisms in individual methods. Teaching texts also consist of practical laboratory exercises, in which students can try out the real application of the studied electrochemical methods.

The practical tasks are focused primarily on the demonstration of research that is carried out at our workplace. Students will be able to try, for example, electrochemical modification of the electrode surface, preparation of electrochemical sensors for the determination of analytes, preparation and characterization of a dye-sensitized solar cell or electrochemical evolution of hydrogen.

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Karel Saksl

Solving crystal structures is the royal discipline of X-ray crystallography. Its primary task, with the exception of defects, is to describe the atomic structure of the motif that, by its repetition, fills the volume of the entire crystal or crystalline phase. This task is nowadays more or less routine for single-crystal X-ray diffraction, which can locate hundreds to thousands of non-hydrogen atoms in large unit cells. However, in real practice, we often have material available only in powder form instead of single crystals. Solving the atomic structure from its X-ray diffraction data is non-trivial, mainly because the three-dimensional diffraction space of a single crystal is reduced to one dimension by measuring a large number of randomly oriented microcrystals (crystallites). Therefore, the solution itself requires, in addition to proper measurement methodology, the selection of suitable tools, procedures, and strategies that, through optimization, will lead to the solution and refinement of the given crystalline phase. The current limit of this method is approximately 100 non-hydrogen atoms in the asymmetric part of the unit cell, which, however, is sufficient for most inorganic materials.

The goal of these educational texts is to provide students in the second and third levels of university studies with specific guidance on solving crystal structures from powder X-ray diffraction data. These scripts build upon my first monograph and require practical knowledge of its content. Similar to my previous monograph, I offer solved examples without a deep theoretical introduction, demonstrating procedures and strategies leading to the correct solution of crystalline phases using the freely available GSAS-II program. The examples are arranged from simpler to more complex, and the reader will find many useful pieces of information in the literature references as well as in the comments below the line. Part of these scripts are data intended for your individual practice of the described procedures. 

Karel Sakls

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