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Praktické cvičenia z röntgenovej difraktometrie
E-book
The aim of these study texts is to provide students in the second and third levels of higher education with specific guidance on processing 2D diffraction data, performing phase analysis from X-ray diffraction data, and refining microstructural parameters of identified phases using the Rietveld refinement method.
This guide is designed in the form of real-world tasks from materials research and leads the reader step by step through the processes of processing, evaluating, and interpreting the measured data. For this purpose, freely accessible programs such as Fit2D, QualX, POV-Ray, and GSAS II will be used, as well as a freely downloadable commercial program (Diamond) that allows for task execution in demonstration mode. Phase analysis will be conducted exclusively using the freely distributable crystallographic database Crystallography Open Database (COD).