POROUS MATERIALS FOR ENVIRONMENTAL APPLICATIONS 2024

E-book

Jozef Bednarčík

Crystallography deals with discerning the arrangement and bonding of atoms in crystalline solids. Almost immediately after their discovery, X-rays began to be used to study the internal structure of substances.

The first chapter of this textbook deals with the basic concepts of crystallography. At the beginning, crystalline solids are characterized. In the next section, the basic types of bonds and their characteristics are briefly presented. The main subject of this chapter is the interpretation of basic concepts such as symmetry operations, translational periodicity, grid, elementary cell. Spatial lattices and crystal systems are presented. At the end of this chapter, attention is paid to the description of individual types of defects in crystal structures. In the second chapter, the Bohr model of the hydrogen atom is presented. Individual quantum numbers and their meaning are given.

Next, energy levels and allowed transitions within an atom with multiple electrons are described. The second chapter concludes with the characterization of the basic absorption and emission processes. The third chapter is devoted to the production of X-ray radiation and its properties. Sources of X-ray radiation and a description of their operation are presented.

Interaction of X-ray radiation with matter, absorption and detection of X-ray radiation are the subject of the last part of this chapter.

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E-book

Karel Saksl

The aim of these study texts is to provide students in the second and third levels of higher education with specific guidance on processing 2D diffraction data, performing phase analysis from X-ray diffraction data, and refining microstructural parameters of identified phases using the Rietveld refinement method.

This guide is designed in the form of real-world tasks from materials research and leads the reader step by step through the processes of processing, evaluating, and interpreting the measured data. For this purpose, freely accessible programs such as Fit2D, QualX, POV-Ray, and GSAS II will be used, as well as a freely downloadable commercial program (Diamond) that allows for task execution in demonstration mode. Phase analysis will be conducted exclusively using the freely distributable crystallographic database Crystallography Open Database (COD).

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E-book

Mária Vilková - Monika Garberová - Michal Goga

Nuclear Magnetic Resonance (NMR) is currently a widely used analytical tool that finds application in many fields of science and technology. The broadening of its practical use brings with it the necessity to create educational texts appropriate to the given scientific discipline.

This university textbook is intended for students of biology and serves as a supplement to the study materials for the advanced master's course "Biology of Lichens." At the same time, it represents a useful resource for master's and doctoral students involved in research, helping them interpret NMR spectra and present basic theoretical concepts.

The textbook briefly describes the important aspects of each NMR spectroscopic technique without delving excessively into the physical principles of individual methods or complex mathematical analyses. In this edition, the structures of lichen metabolites have been included, which students will isolate, purify, and identify using various analytical methods during practical exercises. An entire chapter is dedicated to a detailed description of solving the NMR spectra of isolated metabolites, with each step in elucidating the structures of both known and unknown metabolites explained in detail. The solved tasks are followed by numerous unsolved examples, including high-resolution 1D and 2D NMR spectra of metabolites, intended to further develop the acquired knowledge and skills of students and doctoral candidates in structure elucidation using NMR spectroscopy.

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E-publication

Beáta Valkay ed.
Ivana Slepáková-Monika Balogová a kol.

EFFUSE - Scientific Education for Advanced is an educational material designed for university students interested in ecological sciences, biology and environmental protection. The publication was developed as part of the EFFUSE project and focuses on the scientific investigation of living organisms in the river ecosystem, with an emphasis on their ecological role and importance as bioindicators. The river ecosystem is a dynamic environment where a wide range of organisms can be studied, from algae and phytoplankton to aquatic invertebrates, fish, amphibians and reptiles. This publication presents a detailed study of their adaptations, life cycles, reproductive strategies and their importance for ecological balance. Particular attention is paid to fish and amphibians, whose environmental demands and sensitivity to pollution make them important indicators of water quality and environmental status. The publication also provides guidance on how to integrate their study into university education in the form of practical research. It also includes a chapter on science education in the context of sustainable development, which is often absent from university curricula in Slovakia and Ukraine. This material promotes the link between theory and practice and develops students' scientific thinking in order to prepare them to meet the environmental challenges of the future.

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