NOVEL TRENDS IN CHEMISTRY, RESEARCH AND EDUCATION at the Faculty of Science of Pavol Jozef Šafárik University in Košice 2023

E-book

Miroslav Almáši

The scientific book of abstracts from the conference „Novel Trends in Chemistry, Research and Education 2023“ is a summary of the contributions of conference participants, which contain the original results of their scientific and research activities.

The contributions published in this volume can be divided according to content into the fields of analytical, inorganic, organic, physical chemistry, biochemistry, didactics of chemistry, and NMR spectroscopy.

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Quantity

978-80-574-0246-6

Data sheet

Method of publication:
E-book (pdf)
Editor:
Miroslav Almáši
Document type:
Book of abstracts
Number of pages:
102
Available from:
22.11.2023
Year of publication:
2023
Edition:
1st edition
Publication language:
English
Faculty:
Prírodovedecká fakulta
License:
CC BY NC ND (Uveďte autora - Nepoužívajte komerčne - Nespracovávajte)
- Free for download

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New Trends in Chemistry, Research and Education...

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The scientific book of abstracts is a summary of the contributions of teachers, scientists and other conference participants, which contain the original results of their scientific and research activities. Their work will be the subject of the next domestic conference „New Trends in Chemistry, Research and Education at Faculty of Science of P. J. Šafárik University in Košice 2020“. The conference is a space for dialogue between scientific academics on the one hand and professional staff and students on the other.

The contributions published in this volume can be divided according to content into the field of analytical, inorganic, physical, organic chemistry, biochemistry and didactics of chemistry. All contributions are interesting and can be used in further creative scientific and research work, in the process of education and in practical work.

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These "Exercise Manuals" present a concise overview of commonly used methodologies as well as progressive techniques, such as the use of liquid chromatography and fluorescence microscopy. Individual tasks were selected based on the research focus of the Department of Botany at the Faculty of Science, Pavol Jozef Šafárik University in Košice, particularly in the context of "stress physiology."

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Vybrané kapitoly z koloidnej chémie

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Working with this study text requires adequate knowledge of physical chemistry, physics, and biology, as navigating the presented material becomes challenging without this foundation. A solid grasp of mathematics is essential and aids in understanding colloidal chemistry problems. The textbook, structured into individual chapters, first addresses optical and molecular-kinetic properties after classifying and characterizing disperse systems.

This university-level textbook is primarily intended for students in chemical and ecological disciplines at the Faculty of Science, Pavol Jozef Šafárik University in Košice. It does not aim to exhaustively cover every detail of the subject, as comprehensive treatments are already available in specialized monographs on colloid and macromolecular chemistry, as well as in foundational physical chemistry textbooks.

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Praktické cvičenia z röntgenovej difraktometrie II

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Solving crystal structures is the royal discipline of X-ray crystallography. Its primary task, with the exception of defects, is to describe the atomic structure of the motif that, by its repetition, fills the volume of the entire crystal or crystalline phase. This task is nowadays more or less routine for single-crystal X-ray diffraction, which can locate hundreds to thousands of non-hydrogen atoms in large unit cells. However, in real practice, we often have material available only in powder form instead of single crystals. Solving the atomic structure from its X-ray diffraction data is non-trivial, mainly because the three-dimensional diffraction space of a single crystal is reduced to one dimension by measuring a large number of randomly oriented microcrystals (crystallites). Therefore, the solution itself requires, in addition to proper measurement methodology, the selection of suitable tools, procedures, and strategies that, through optimization, will lead to the solution and refinement of the given crystalline phase. The current limit of this method is approximately 100 non-hydrogen atoms in the asymmetric part of the unit cell, which, however, is sufficient for most inorganic materials.

The goal of these educational texts is to provide students in the second and third levels of university studies with specific guidance on solving crystal structures from powder X-ray diffraction data. These scripts build upon my first monograph and require practical knowledge of its content. Similar to my previous monograph, I offer solved examples without a deep theoretical introduction, demonstrating procedures and strategies leading to the correct solution of crystalline phases using the freely available GSAS-II program. The examples are arranged from simpler to more complex, and the reader will find many useful pieces of information in the literature references as well as in the comments below the line. Part of these scripts are data intended for your individual practice of the described procedures. 

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