Praktické cvičenia z röntgenovej difraktometrie II

E-book

Karel Saksl

Solving crystal structures is the royal discipline of X-ray crystallography. Its primary task, with the exception of defects, is to describe the atomic structure of the motif that, by its repetition, fills the volume of the entire crystal or crystalline phase. This task is nowadays more or less routine for single-crystal X-ray diffraction, which can locate hundreds to thousands of non-hydrogen atoms in large unit cells. However, in real practice, we often have material available only in powder form instead of single crystals. Solving the atomic structure from its X-ray diffraction data is non-trivial, mainly because the three-dimensional diffraction space of a single crystal is reduced to one dimension by measuring a large number of randomly oriented microcrystals (crystallites). Therefore, the solution itself requires, in addition to proper measurement methodology, the selection of suitable tools, procedures, and strategies that, through optimization, will lead to the solution and refinement of the given crystalline phase. The current limit of this method is approximately 100 non-hydrogen atoms in the asymmetric part of the unit cell, which, however, is sufficient for most inorganic materials.

The goal of these educational texts is to provide students in the second and third levels of university studies with specific guidance on solving crystal structures from powder X-ray diffraction data. These scripts build upon my first monograph and require practical knowledge of its content. Similar to my previous monograph, I offer solved examples without a deep theoretical introduction, demonstrating procedures and strategies leading to the correct solution of crystalline phases using the freely available GSAS-II program. The examples are arranged from simpler to more complex, and the reader will find many useful pieces of information in the literature references as well as in the comments below the line. Part of these scripts are data intended for your individual practice of the described procedures. 

Karel Sakls

Download the e-book for free  (pdf)

Quantity

978-80-574-0090-5

Data sheet

Method of publication:
E-book (pdf)
Author:
Karel Saksl
Document type:
Course Notes
Number of pages:
143
Available from:
05.04.2022
Year of publication:
2022
Edition:
1st edition
Publication language:
Slovak
Faculty:
Prírodovedecká fakulta
License:
Creative Commons BY NC ND (Uveďte autora - Nepoužívajte komerčne - Nespracovávajte)
DOI:
https://doi.org/10.33542/CRD2022-0090-5
- Free for download

4 other products in the same category:

Geografické poznatky bez hraníc - výber z maďarských a slovenských príspevkov z fyzickej a humánnej geografie.

Geografické poznatky bez hraníc - výber z...

E-book

E-book

Dušan Barabas a kol.

The presented text is the final product of work within the project "Tanuljunk egymástól!/Let’s Learn from Each Other!" The project emerged from long-standing contacts between the staff of the Centre for Regional Studies of the Hungarian Academy of Sciences and the Institute of Geography at the Faculty of Science, Pavol Jozef Šafárik University in Košice, as a natural effort to expand mutual cooperation. The first step was collaboration within Interreg II projects, involving a broad range of institutions from both academic and non-academic environments. This initial attempt was unsuccessful due to administrative errors. Consequently, a project titled HUSK/0801/1.6.1/0003 "Tanuljunk egymástól!/Let’s Learn from Each Other!" was prepared and developed in agreement with the Hungarian side. It was approved and co-financed by the European Regional Development Fund under the Hungary-Slovakia Cross-Border Cooperation Program 2007–2013.

Download the e-book for free (pdf)

Výpočtová a kognitívna neuroveda II (Návody na cvičenia)

Výpočtová a kognitívna neuroveda II (Návody na...

E-book

E-book

Norbert Kopčo

Neuroscience is an interdisciplinary field of science at the interface of biological, psychological and computer sciences, which aims to describe the functioning of the brain and mind. Computational and cognitive neuroscience are subfields of neuroscience focused on the study of information processing in the human and animal nervous systems, and on the theoretical description of the brain and mind. This university textbook contains several assignments that provide an overview of the methods used in computational and cognitive neuroscience, with an emphasis on mathematical modeling and on the behavioral study of cognitive processes. The textbook builds on the author's previous works.

Download e-book for free (pdf)

School of XFEL and Synchrotron Radiation Users – SFEL 2024

School of XFEL and Synchrotron Radiation Users...

E-book

E-book

Jozef Bednarčík (ed.)

Pavol Jozef Šafárik University in Košice under the auspices of Ministry of Education, Research, Development and Youth of the Slovak Republic, Ministry of Economy of the Slovak Republic and European X-Ray Free-Electron Laser Facility GmbH in Hamburg organizes School of XFEL and Synchrotron Radiation Users 2024 (SFEL 2024). The school is continuation of the Winter Schools of Synchrotron radiation held in 2011, 2013, 2014 and SFEL 2017, 2018, 2019 and 2022. The aim of the SFEL2024 school is to facilitate the growth of new Slovak research community of high expertise in high-efficiency RTG laser and synchrotron and neutron sources. The SFEL school is designed for efficient transfer of the rapidly developing know-how in these areas to young generation – researchers and university students. The next aim of the SFEL2024 is strengthening of personal connections between the local Slovak research community and forming scientific teams of XFEL users. Slovak research community thus can take advantage of the fact that Slovakia is a shareholder of European XFEL GmbH Company in Hamburg, but also makes more efficient use of other closely related scientific facilities, including ILL and ESRF in Grenoble and DESY in Hamburg.

Download the e-book for free (pdf)

Nanotechnology

Nanotechnology

€17.68
Availability: 58 In Stock

 Andrej Oriňak - Renáta Oriňaková - Andrea Fedorková

Nanotechnology represent the fastest developing science in the present. They are based on the technologies that enable the matter manipulation at atomic level. Nanotechnology offer prepartion of the new materials with unknown and very specific properties and functions.Recent nanotechnology still stay in formative phase of their development. But more and more they are visible with nano-specific phenomenons in the fundamental control of the properties as well mater behaviour. This is quite possible that without nanotechnology will not work any science to the future, moreover that science will not exist anymore. Nanotechnolgy will give a chance and force to transform world to more environmental and comfortable. Expected is expansion of the nanotechnolgy to molecular nanosystems – heterogenous nets, in which molecules and supramolecules work as the nanodevices. The computers and robots will be reduced to the small and ultrasmall dimensions. In medicine will foremost the application of nanotechnology in genetic therapy and elimination of ageing. Nanosurgery will work at molecular level, cancer cells will be identified early and filtered , then substituted with healthy and unchanged. It is necessary to inform university or high school students  about principles of nanotechnolgy, preparation of the nanostructures, functionality of them and to offer full representation about molecular systems and nanodevices; the methods of nanostructures characterization and about application in miniaturized systems. 

Authors

This website uses cookies to ensure you get the best experience on our website