Praktické cvičenia z röntgenovej difraktometrie II

E-book

Karel Saksl

Solving crystal structures is the royal discipline of X-ray crystallography. Its primary task, with the exception of defects, is to describe the atomic structure of the motif that, by its repetition, fills the volume of the entire crystal or crystalline phase. This task is nowadays more or less routine for single-crystal X-ray diffraction, which can locate hundreds to thousands of non-hydrogen atoms in large unit cells. However, in real practice, we often have material available only in powder form instead of single crystals. Solving the atomic structure from its X-ray diffraction data is non-trivial, mainly because the three-dimensional diffraction space of a single crystal is reduced to one dimension by measuring a large number of randomly oriented microcrystals (crystallites). Therefore, the solution itself requires, in addition to proper measurement methodology, the selection of suitable tools, procedures, and strategies that, through optimization, will lead to the solution and refinement of the given crystalline phase. The current limit of this method is approximately 100 non-hydrogen atoms in the asymmetric part of the unit cell, which, however, is sufficient for most inorganic materials.

The goal of these educational texts is to provide students in the second and third levels of university studies with specific guidance on solving crystal structures from powder X-ray diffraction data. These scripts build upon my first monograph and require practical knowledge of its content. Similar to my previous monograph, I offer solved examples without a deep theoretical introduction, demonstrating procedures and strategies leading to the correct solution of crystalline phases using the freely available GSAS-II program. The examples are arranged from simpler to more complex, and the reader will find many useful pieces of information in the literature references as well as in the comments below the line. Part of these scripts are data intended for your individual practice of the described procedures. 

Karel Sakls

Download the e-book for free  (pdf)

Quantity

978-80-574-0090-5

Data sheet

Method of publication:
E-book (pdf)
Author:
Karel Saksl
Document type:
Course Notes
Number of pages:
143
Available from:
05.04.2022
Year of publication:
2022
Edition:
1st edition
Publication language:
Slovak
Faculty:
Prírodovedecká fakulta
License:
Creative Commons BY NC ND (Uveďte autora - Nepoužívajte komerčne - Nespracovávajte)
DOI:
https://doi.org/10.33542/CRD2022-0090-5
- Free for download

16 other products in the same category:

TEXTBOOK OF MEDICAL CHEMISTRY

E-book

E-book

Lucia Andrezálová, Zdeňka Ďuračková,Mária Chomová,Vladimír Jakuš, Miriam Ježovičová, Jana Muchová, Zuzana Országhová,Ingrid Žitňanová

Chemistry and biochemistry at medical faculties are integral parts of basic theoretic knowledge of contemporary graduate. Educational book “Textbook of Medical Chemistry” is destined to students of study branches General Medicine and Dentistry for the course “Medical Chemistry”.

It is structured into 13 chapters concerning several topics: general and physical chemistry, organic chemistry, chemistry of natural substances (static biochemistry), enzymology and oxidative stress.

Individual chapters provide comprehensible explanation of the fundamentals of physico-chemical, chemical and biochemical relationships applying in living systems as well as the knowledge of the structure of biologically important molecules (simple molecules and macromolecules) related to their properties and biological function.

Download e-book for free (pdf)

Cvičenia z imunológie

E-book

E-book

Vlasta DemečkováPetra HradickáPetra Adamková

The learning material for the course Practice in Immunology is based on several years of experience with teaching this subject, but mainly to provide students from the Biology Department at the Faculty of Natural Sciences, UPJŠ in Košice with sufficient theoretical background for practical exercises. It also serves as a scientific diary for detailed recording of all experimental data necessary for preparing laboratory protocols from individual exercises.

In studying biology, it is essential that students thoroughly understand not only the basics of each discipline but also acquire practical skills, including designing scientific experiments, selecting appropriate analytical/investigative techniques up to interpreting and presenting experimental data. The goal of this new publication is therefore to provide master's students with a practical study guide that supports and expands their knowledge about basic immunology principles.

Download e-book for free (pdf)

Študentská vedecká konferencia PF UPJŠ 2018

E-book

E-book

Katarína Cechlárová (ed.)

In 2018, the Student Scientific Conference was held on April 18, 2018, in 16 sections covering biology and ecology, chemistry, physics, geography, mathematics, computer science, and their subject didactics. There were 110 registered contributions from bachelor's and master's students. Additionally, eight high school students participated outside of the competition; these students already visit our alma mater at a young age, work in our laboratories, and prepare for further studies under the guidance of our enthusiastic teachers. The day also included a programming competition and the IHRA competition in three categories, where students from PF UPJŠ competed alongside pupils from elementary and secondary schools.

The abstracts of the Student Scientific Conference contributions convincingly demonstrate that PF UPJŠ students study their field not only theoretically but also actively engage in solving partial scientific problems that are part of the research goals at PF UPJŠ institutes. This collection provides an overview of scientific activity at the faculty, which we believe will be interesting for the broader public as well.

Download the e-book for free  (pdf)

48th Conference of the Middle European...

E-book

E-book

Jozef Strečka,Katarína Karľová

The 48th Conference of the Middle European Cooperation in Statistical Physics (MECO48) will be held on May 22nd-26th, 2023, in Stará Lesná, High Tatras, Slovakia. The MECO48 conference continues a long tradition of regular international meetings in the domain of statistical physics established in the early 1970s with the aim of bridging the gap between the communities of scientists from the Eastern and Western parts of Europe separated by the iron curtain.

In the modern era the MECO conferences attract attention of the community of scientists who are active in the field of statistical physics including various interdisciplinary applications to biology, medicine, geography, finance, quantum information theory, and machine learning.

The MECO48 conference is organized jointly by Faculty of Science of Pavol Jozef Šafárik University in Košice, Institute of Experimental Physics of Slovak Academy of Sciences in Košice, Institute of Physics, Slovak Academy of Sciences in Bratislava and Faculty of Humanities and Natural Sciences, University of Prešov under the financial support of Slovak Research and Development Agency (grant No. APVV-20-0150) and other sponsors.

Download e-book for free (pdf)

Teória efektívneho poľa pre lokalizované...

E-book

E-book

Michal Jaščur

This monograph is devoted to the discussion of effective field theory based on the differential operator method, originally introduced by Honmura and Kaneyoshi in 1979, which remains actively used for theoretical studies of localized spin models of magnetism—particularly variants of the Ising model. To date, this methodology has been applied by numerous authors to investigate a wide range of systems, including crystalline systems, diluted magnetic systems, systems with random exchange interactions, amorphous magnetic materials, systems under random magnetic and crystalline fields, thin magnetic layers, magnetic systems with free surfaces, binary and ternary magnetic alloys, among others.

During my scientific career, I have collaborated with several leading experts in this field—including Prof. Kaneyoshi, with whom I completed two long-term research stays—to advance the development of the differential operator method (and consequently effective field theory). Within this research area, I have published over 40 scientific papers in prominent international physics journals. These works include both methodological advancements and significant applications that predict intriguing physical phenomena, such as multicompensation phenomena in ferrimagnets.

Download the e-book for free

Návody na praktické cvičenia z biotechnológie

E-book

E-book

Danica Sabolová

This university textbook is intended for students of the Faculty of Science of the University of Applied Sciences in Košice who have enrolled in practical exercises in Biotechnology, but also for all other students who are interested in learning about the practical applications of biotechnology.

The aim of the practical course is to familiarize students with basic biotechnological methods and their applications. The students will verify in practice the theoretical knowledge acquired in the Biotechnology lectures such as the course of fermentation processes, wine production, preparation of fermented milk products and cheese, preparation of culture media, inoculation and cultivation of microorganisms, etc. The practical exercises also include the use of analytical and spectral methods, which are an integral part of biochemistry.

The scripts are published only in electronic form and are available on the University's website: http://kosice.upjs.sk/~kbch/sk, for the reason that it will always be possible to update and modernize the content of the laboratory exercises.

Download the e-book for free (pdf)

Biológia kryptogamov

E-book

E-publication
Michal Goga-Marko S. Sabovljević-Martin Bačkor-Dajana Kecsey-Deepti Routray
A comprehensive guide that introduces you to the fascinating diversity and systematics of lower plants. These practical lessons are designed to provide hands-on training, allowing students to engage directly with the interesting study of Cryptogams by observation, analysis, and identification and experimentation. Beginning with the overall idea of cryptogam in a field trip near by the vicinity of Botanical garden then followed by the basics of microscopy in, will help to gain essential skills in understanding the components and proper usage of a microscope, a fundamental tool in botanical studies.
Download the e-book for free (pdf)

Ortuť v životnom prostredí ako rizikový faktor...

€9.04
Availability: 10 In Stock

Tatiana Kimáková

Táto vedecká monografia je komplexnou vedeckou prácou zameranou na prítomnosť a pôsobenie ortuti v životnom prostredí, ale aj na rizikové faktory zdravia, ktoré sú s ňou spojené. Monografia predstavuje charakteristiku ortuti v multidisciplinárnom zábere, prezentuje využitie v priemysle a v zdravotníctve, popisuje negatívne vplyvy ortuti v životnom prostredí, na zdravotný stav obyvateľstva. Zároveň prináša návrhy a odporúčania pre rizikové skupiny ľudí. Súčasťou monografie je komplexný výskum koncentrácie ortuti vo vzorkách komodít domácej i zahraničnej produkcie a vo vzorkách rastlín pomocou atómového absorpčného spektrometra AMA 254. Vedecká monografia je vhodná pre vedeckú komunitu, študentov medicínskych, veterinárnych, prírodovedných a poľnohospodárskych odborov ako aj pre študentov verejného zdravotníctva všetkých troch stupňov vysokoškolského štúdia. Monografia je učená aj pre všetkých záujemcov z radov informovanej verejnosti.

Autorka

Štruktúra a reaktivita – riešené príklady a...

E-book

E-book

Slávka Hamuľaková

The textbook "Structure and reactivity - solved examples and tasks, part 1" is the basis for teaching the subject "Structure and reactivity" for students of the 1st year of master's studies at the Faculty of Science, UPJŠ, department of Organic Chemistry. The textbook is divided into individual chapters, each chapter offering students examples of chemical reactions, where their course is explained on the basis of appropriate reaction mechanisms. A substantial part of the textbook consists of unresolved tasks, the main goal of which is the development of students' knowledge and skills. Due to the fact that the textbook is focused on only one semester of study, it cannot cover all reactions, rather it is only representative examples of different types of reactions, such as: addition reactions, elimination reactions, aromatic substitution, addition-elimination reactions, radical reactions and pericyclic reactions.

Download the e-book for free (pdf)

Exactly Solvable Models in Statistical Physics

E-book

E-book

Jozef Strečka

The present textbook deals with exactly solved models and their diverse applications in several branches of physics such as mathematical physics, statistical physics, condensed matter physics and so on. Exactly soluble models are currently considered as an inspiring research field in its own right, which regrettably requires a considerable knowledge of sophisticated mathematics. Accordingly, my primary ambition was to provide an intro- ductory course for undergraduate students that would cover the simplest exactly solved models, whose rigorous solutions are available even after modest calculation. The present textbook should be therefore regarded as an auxiliary graduate-level textbook, which should serve as the student’s guide on this beautiful but surely intricate subject.

Download the e-book for free (pdf)

Zbierka príkladov z atómovej a jadrovej fyziky

E-book

E-book

Janka Vrláková - Adela Kravčáková - Stanislav Vokál

The presented "Collection of Problems in Atomic and Nuclear Physics" is intended as a basic study material for lectures in General Physics IV in the second year of the bachelor's single-subject physics program and interdisciplinary studies combined with physics at the Faculty of Science of P. J. Šafárik University in Košice.

Its aim is to support independent student work and to deepen the acquired knowledge from the given physics course by solving selected problems. It is divided into three main parts: Atomic Physics, Nuclear Physics, and Experimental Methods of Nuclear Physics.

Each thematic chapter contains an overview of basic concepts, relations, and formulas necessary for better understanding of sample problems and for solving the attached set of unsolved problems.

Download the e-book for free (pdf)

The 9th International Conference on Novel...

E-book

E-publication

Soňa Király

The Book of Abstracts of The 9th International Conference on Novel Materials Fundamentals and Applications, NFA 2025, contains 46 contributions from the participants of this conference. This congress is primarily focused on novel materials, ranging from theory to practical applications, with the aim of demonstrating how fundamental discoveries can lead to innovative implementations. All contributions are inspiring and professionally prepared.

Download the e-book for free (pdf)

This website uses cookies to ensure you get the best experience on our website