Štúdium fyzikálnych vlastností tuhých látok

E-book

Karel Saksl

Solving crystal structures is the royal discipline of X-ray crystallography. Its primary task, with the exception of defects, is to describe the atomic structure of the motif that, by its repetition, fills the volume of the entire crystal or crystalline phase. This task is nowadays more or less routine for single-crystal X-ray diffraction, which can locate hundreds to thousands of non-hydrogen atoms in large unit cells. However, in real practice, we often have material available only in powder form instead of single crystals. Solving the atomic structure from its X-ray diffraction data is non-trivial, mainly because the three-dimensional diffraction space of a single crystal is reduced to one dimension by measuring a large number of randomly oriented microcrystals (crystallites). Therefore, the solution itself requires, in addition to proper measurement methodology, the selection of suitable tools, procedures, and strategies that, through optimization, will lead to the solution and refinement of the given crystalline phase. The current limit of this method is approximately 100 non-hydrogen atoms in the asymmetric part of the unit cell, which, however, is sufficient for most inorganic materials.

The goal of these educational texts is to provide students in the second and third levels of university studies with specific guidance on solving crystal structures from powder X-ray diffraction data. These scripts build upon my first monograph and require practical knowledge of its content. Similar to my previous monograph, I offer solved examples without a deep theoretical introduction, demonstrating procedures and strategies leading to the correct solution of crystalline phases using the freely available GSAS-II program. The examples are arranged from simpler to more complex, and the reader will find many useful pieces of information in the literature references as well as in the comments below the line. Part of these scripts are data intended for your individual practice of the described procedures. 

Karel Sakls

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E-book

Andrej Mock

The structure of the animal body is extremely varied. Each species has its distinctive morphological features, which bears as a testimony to long-term development and belonging to the developmental lineage. At the same time, the body has been tested for a long time by natural conditions, resulting in unique adaptations to the environment and life strategy. Despite this admirable variety - which includes both recent and fossil animals and which we have far from mapped – a comparison of body parts brings knowledge we can generalize: the main building principles, and boundaries within which phenotypic diversity is realized.

Comparative animal morphology today uses the latest methodological material and knowledge from other disciplines, from genetics, molecular biology and experimental embryology, through progressive imaging methods (e.g. electron microscopy, computer micro-tomography) and the possibilities of subsequent software processing of image material (measurement, staining, etc.) to the view of physics, chemistry, statics and geometry on the structures (to nanostructures) of the living body. Detailed knowledge of historical and contemporary conditions on Earth is an important interpretative context in the study of animal morphology. Surprisingly, the knowledge accumulated after centuries of research is now rapidly supplemented by new knowledge, and often the traditional knowledge is subsequently reinterpreted. Finally, and no less important, in studying animal (and human) morphology, we learn surprising knowledge about ourselves.

The author of the presented textbook had the ambition in a simplified form to introduce the reader, especially the student of biological studies, into a dynamic and fascinating scientific discipline, as the current comparative animal morphology is.

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E-publication
Michal Goga-Marko S. Sabovljević-Martin Bačkor-Dajana Kecsey-Deepti Routray
A comprehensive guide that introduces you to the fascinating diversity and systematics of lower plants. These practical lessons are designed to provide hands-on training, allowing students to engage directly with the interesting study of Cryptogams by observation, analysis, and identification and experimentation. Beginning with the overall idea of cryptogam in a field trip near by the vicinity of Botanical garden then followed by the basics of microscopy in, will help to gain essential skills in understanding the components and proper usage of a microscope, a fundamental tool in botanical studies.
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E-book

Vladimír Komanický

The aim of this textbook is to acquaint students in physics, chemistry and material science on both undergraduate and graduate level, with the techniques used to prepare micro-electromechanical devices, nanoobjects and nanostructures using the so called top down methodologies. The is no requirement for this course to pass any prior courses. The introduction part of the text defines the forces that affect nanoobjects and the interactions between them. Reader can understand in detail why properties of nanomaterials and nanostructures are so different when comprared to their macroscopic counterparts. Text gives also an overview of thin film preparation technologies as precursors for the preparation of nanostructures. The main emphasis in Volume I is on conventional lithographic technologies for the preparation and shaping of nanostructures, methods for characterization of thin films, nanoparticles and nanomaterials. Unconventional lithographic methods will also be discussed in the prepared upcoming Volume II. Student will also get acquainted with the applications of nanostructures in research focused on nanophysics, nanocatalysis and nanoelectronics. The textbook is used as a study material for the course ÚFV / MPN / 14 - Methods of preparation and characterization of nanostructures. Part of the course is also a laboratory exercise in which the student gets acquainted with the techiques used for the preparation and characterization of thin films and top-down technologies used for the preparation of nanostructures.

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