Novel Trends in Chemistry, Research and Education 2025

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Miroslav Almáši

The scientific book of abstracts from the conference „Novel Trends in Chemistry, Research and Education 2023“ is a summary of the contributions of conference participants, which contain the original results of their scientific and research activities.

The contributions published in this volume can be divided according to content into the fields of analytical, inorganic, organic, physical chemistry, biochemistry, didactics of chemistry, and NMR spectroscopy.

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Danica Sabolová

This university textbook is intended for students of the Faculty of Science of the University of Applied Sciences in Košice who have enrolled in practical exercises in Biotechnology, but also for all other students who are interested in learning about the practical applications of biotechnology.

The aim of the practical course is to familiarize students with basic biotechnological methods and their applications. The students will verify in practice the theoretical knowledge acquired in the Biotechnology lectures such as the course of fermentation processes, wine production, preparation of fermented milk products and cheese, preparation of culture media, inoculation and cultivation of microorganisms, etc. The practical exercises also include the use of analytical and spectral methods, which are an integral part of biochemistry.

The scripts are published only in electronic form and are available on the University's website: http://kosice.upjs.sk/~kbch/sk, for the reason that it will always be possible to update and modernize the content of the laboratory exercises.

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Karel Saksl

Solving crystal structures is the royal discipline of X-ray crystallography. Its primary task, with the exception of defects, is to describe the atomic structure of the motif that, by its repetition, fills the volume of the entire crystal or crystalline phase. This task is nowadays more or less routine for single-crystal X-ray diffraction, which can locate hundreds to thousands of non-hydrogen atoms in large unit cells. However, in real practice, we often have material available only in powder form instead of single crystals. Solving the atomic structure from its X-ray diffraction data is non-trivial, mainly because the three-dimensional diffraction space of a single crystal is reduced to one dimension by measuring a large number of randomly oriented microcrystals (crystallites). Therefore, the solution itself requires, in addition to proper measurement methodology, the selection of suitable tools, procedures, and strategies that, through optimization, will lead to the solution and refinement of the given crystalline phase. The current limit of this method is approximately 100 non-hydrogen atoms in the asymmetric part of the unit cell, which, however, is sufficient for most inorganic materials.

The goal of these educational texts is to provide students in the second and third levels of university studies with specific guidance on solving crystal structures from powder X-ray diffraction data. These scripts build upon my first monograph and require practical knowledge of its content. Similar to my previous monograph, I offer solved examples without a deep theoretical introduction, demonstrating procedures and strategies leading to the correct solution of crystalline phases using the freely available GSAS-II program. The examples are arranged from simpler to more complex, and the reader will find many useful pieces of information in the literature references as well as in the comments below the line. Part of these scripts are data intended for your individual practice of the described procedures. 

Karel Sakls

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Božena Mihalíková - Ondrej Hutník - Jozef Kiseľák

The textbook is devoted to the mathematical analysis of infinite series of numbers and functions. It is intended for students of mathematics, physics and computer science, as well as interdisciplinary study of combination with mathematics. It contains a theoretical background for investigating the convergence of infinite series, expanding functions into power and Taylor series, as well as the use of these results in various problems of mathematics, physics, and computer science. Using the historical background the textbook clarifies the motivations and the need to introduce some key concepts and their further development. Basic concepts and statements are demonstrated on a large number of solved exercises, but it contains a number of exercises for independent practice. Several results are supplemented by dynamic animations executable in the electronic version of the textbook.

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Andrea Morovská Turoňová - Renáta Oriňaková - František Kaľavský 

The university textbooks "Practical Exercises in Physical Chemistry" are intended as teaching literature for students of the 2nd year of the Chemistry study program and the 3rd year of the interdisciplinary study program at the Faculty of Science of the Pavel Jozef Šafárik University in Košice.

The three chapters summarize the basic knowledge of thermodynamics, electrochemistry and kinetics, the next chapter deals with the measurement of some other physico-chemical quantities. The tasks developed on the basis of cooperation with the Criminalistics and Expertise Institute of the Police in Košice, which also participates in the innovation of practical teaching, are also very attractive and interesting for students. Thematic units are updated and supplemented by new knowledge, principles as well as detailed working procedures using new instrumentation.

The aim of laboratory exercises in physical chemistry is to illustrate and confirm the physicochemical laws and correlations that apply to the quantitative description of chemical phenomena. Students will learn to use instruments and equipment that occur in physico-chemical laboratories, they will learn the principles of accurate and correct quantitative measurement of physical quantities, important from a chemical point of view. They can also develop professional and scientific communication skills, and we want to support their creative approach to making measurement protocols.

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Ondrej Krídlo

University textbooks present the basics of knowledge systems, which are divided into two parts. The first part of the publication is devoted to the basis of Formal Concept Analysis, ie the method of data analysis, knowledge representation and information processing, which is based on the formalization of the concept. In the second part we deal with the basics of logic programming, procedural semantics of logic programming, ie programs - theories, questions, SLD-derivation, SLD-tree, search strategies.

University textbooks are intended for students of master's degree programs in computer science.

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Adriana Zeleňáková - Jozef Bednarčík

Peer-reviewed Proceedings of the Scientific Conference NANOVIR

The main objective of the scientific conference NANOVIR was the presentation of scientific results obtained during the implementation of the NANOVIR project – Nanoparticles for solving diagnostic and therapeutic problems with COVID-19, co-financed by the European Regional Development Fund within the Operational Programme Integrated Infrastructure 2014 – 2020, ITMS: 313011AUW7.

The project was carried out from January 1, 2021, to June 30, 2023, and was supported with a sum of EUR 1,916,004.79. Three co-investigating organizations participated in the project: Pavol Jozef Šafárik University in Košice as the main investigator, the University of Veterinary Medicine and Pharmacy in Košice as partner no. 1, and the Institute of Experimental Physics of the Slovak Academy of Sciences as partner no. 2.

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Miroslav Almáši (ed.)

The book of abstracts from the conference "Porous Materials for Environmental Applications 2024" is a collection of contributions of the conference participants, which contain original results of their scientific and research activities. The conference was aimed to share new findings dealing with the preparation, characterization and application of porous materials in environmental fields.

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Mária Vilková - Monika Garberová - Michal Goga

Nuclear Magnetic Resonance (NMR) is currently a widely used analytical tool that finds application in many fields of science and technology. The broadening of its practical use brings with it the necessity to create educational texts appropriate to the given scientific discipline.

This university textbook is intended for students of biology and serves as a supplement to the study materials for the advanced master's course "Biology of Lichens." At the same time, it represents a useful resource for master's and doctoral students involved in research, helping them interpret NMR spectra and present basic theoretical concepts.

The textbook briefly describes the important aspects of each NMR spectroscopic technique without delving excessively into the physical principles of individual methods or complex mathematical analyses. In this edition, the structures of lichen metabolites have been included, which students will isolate, purify, and identify using various analytical methods during practical exercises. An entire chapter is dedicated to a detailed description of solving the NMR spectra of isolated metabolites, with each step in elucidating the structures of both known and unknown metabolites explained in detail. The solved tasks are followed by numerous unsolved examples, including high-resolution 1D and 2D NMR spectra of metabolites, intended to further develop the acquired knowledge and skills of students and doctoral candidates in structure elucidation using NMR spectroscopy.

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Ľubomír Kováč

Učebný text „Zoogeografia“ objasňuje základné princípy a historický vývoj rozšírenia živočíchov na Zemi, a ďalej analyzuje faktory, ktoré ho ovplyvňujú. Vďaka moderným vedeckým metódam a technikám výskumu je zoogeografia veľmi dynamicky sa rozvíjajúcou disciplínou. Z geologických etáp je podrobnejšie spracovaná problematika paleoklimatických cyklov kvartéru, holocénu a vývoja postglaciálnej klímy, ktoré zohrali významnú úlohu pri dynamike vývoja živočíšnych areálov. Areálová analýza charakterizuje a triedi areály živočíchov a ich dynamiku v nadväznosti na speciáciu. Podrobne je spracovaná problematika zoogeografických oblastí s dôrazom na palearktickú oblasť. Časť zameraná na dynamickú zoogeografiu rieši najmä problematiku refúgií a reliktov v súvislosti s vývojom pleistocénnej paleoklímy. Text stručnou formou sumarizuje základné antropogénne faktory, ktoré v recentnej dobe drastickým spôsobom limitujú rozšírenie živočíchov v rýchlo ubúdajúcom prírodnom prostredí na Zemi. Text ďalej prehľadným spôsobom charakterizuje biogeografiu Karpát a faunu územia Slovenska. Záverečná časť prezentuje fylogeografiu ako modernú vednú disciplínu zameranú na rekonštrukciu migračných ciest v postglaciáli, ktorá je podložená analýzou molekulárnych markerov populácií živočíchov v širšom geografickom kontexte. 

Autor

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Jozef Bednarčík (ed.)

Pavol Jozef Šafárik University in Košice under the auspices of Ministry of Education, Research, Development and Youth of the Slovak Republic, Ministry of Economy of the Slovak Republic and European X-Ray Free-Electron Laser Facility GmbH in Hamburg organizes School of XFEL and Synchrotron Radiation Users 2024 (SFEL 2024). The school is continuation of the Winter Schools of Synchrotron radiation held in 2011, 2013, 2014 and SFEL 2017, 2018, 2019 and 2022. The aim of the SFEL2024 school is to facilitate the growth of new Slovak research community of high expertise in high-efficiency RTG laser and synchrotron and neutron sources. The SFEL school is designed for efficient transfer of the rapidly developing know-how in these areas to young generation – researchers and university students. The next aim of the SFEL2024 is strengthening of personal connections between the local Slovak research community and forming scientific teams of XFEL users. Slovak research community thus can take advantage of the fact that Slovakia is a shareholder of European XFEL GmbH Company in Hamburg, but also makes more efficient use of other closely related scientific facilities, including ILL and ESRF in Grenoble and DESY in Hamburg.

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Tomáš Samuely

Today, scanning probe microscopes are standard tools in materials science, physics, chemistry, biology, and engineering. Thousands of these microscopes are in operation worldwide and are at least as common and popular as scanning electron microscopes.

Despite the vast number of newer scanning probe microscopy techniques, classical STM remains a significant and irreplaceable method, widely used, for example, in solid-state research. In this text, we will focus on both traditional and innovative STM techniques that are available and utilized in the laboratories of the Center for Low Temperature Physics in Košice.

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Vladimír Zeleňák (ed.)

The proceedings contain contributions from participants of the Student Scientific Conference of the Faculty of Science at UPJŠ in Košice, which took place on April 24, 2014.

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Igor Hudec - Ľubomír Kováč 

The study course provides the basic knowledge on the fundamental parameters, relationships and processes in ecological sciences. Brief content: ecological factors and relations to environment (air, water, soil); influence of ecological factors upon organisms (morphological adaptations, behavioural responses); populations and communities (external and internal parameters of populations, population dynamics); ecosystems (impact assessment) and biomes (basic features and human impact); cycles (hydrologic, gaseous, sedimentation) of basic elements on Earth.  

Authors

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Adriana Zeleňáková

One of the fundamental characteristics of the magnetic state of ferromagnetic materials is the existence of a domain structure. The university textbook "MAGNETIC DOMAINS: SPECIAL PHYSICAL PRACTICE 1" is intended primarily for students of the Master's programme in Physics of Condensed Matter FKLm and for the PhD programme in Progressive Materials PMd within the profile subject Special Practice 1 at the Institute of Physical Sciences of the Faculty of Sciences of the Pavol Jozef Šafárik University in Košice.  The textbook is divided into seven chapters. The first chapter is devoted to the basics of domain theory, including the history of domain observation and the specification of different types of energies in ferromagnetic body. The second chapter presents the relationship between domain structure and magnetisation processes in ferromagnetic materials The third chapter describes the different types of domain-wall interactions with the defect. The fourth chapter illustrates examples of domain structure in selected ferromagnetic body such as grain oriented and non-grain oriented electrical steels, amorphous and nanocrystalline ribbons. The fifth chapter summarises an overview of the different experimental methods used to visualise the domain structure and their advantages or disadvantages with respect to the structure of ferromagnetic materials. The last two chapters, the sixth and the seventh, are devoted to specific experimental tasks for observing the domain structure of a selected polycrystalline sample using the optical microscope Bitter powder method and the MFM (magnetic force microscopy) method. During the preparation of this undergraduate text, its individual parts were developed using the foreign language literature listed in the recommended references.

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Monika Tvrdoňová - Miroslava Martinková

The scientific book of abstracts from conference „Novel Trends in Chemistry, Research and Education 2022“ is a summary of the contributions of conference participants, which contain the original results of their scientific and research activities. The contributions published in this volume can be divided according to content into the field of analytical, inorganic, organic, physical chemistry, biochemistry, didactics of chemistry and NMR spectroscopy.

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